Information card for entry 1517766

Structure parameters

• Formula: C54 H54 N2 Ni O8 P2
• Calculated formula: C54 H52.8 N2 Ni O8 P2
• Title of publication: Monoanionic salicylaldimine ligands with (thio)phosphoryl pendant arms: Synthesis and complexing features
• Authors of publication: Diana V. Aleksanyan; Valentina Yu. Aleksenko; Yulia V. Nelyubina; Andrei A. Vasil-ev; Rinat R. Aysin; Zinaida S. Klemenkova; Vladimir A. Kozlov; Pavel V. Petrovskii; Irina L. Odinets
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2013
• Journal volume: 404
• Pages of publication: 167 - 174
• a: 9.4396 ± 0.0009 Å
• b: 11.8274 ± 0.0011 Å
• c: 12.3009 ± 0.0011 Å
• α: 61.711 ± 0.003°
• β: 76.08 ± 0.002°
• γ: 85.684 ± 0.002°
• Cell volume: 1172.6 ± 0.19 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.087
• Residual factor for significantly intense reflections: 0.0485
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1181
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No