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Information card for entry 1546890
Preview
Coordinates | 1546890.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C52 H70 B2 Ge2 N6 |
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Calculated formula | C52 H70 B2 Ge2 N6 |
Title of publication | Facile activation of alkynes with a boraguanidinato-stabilized germylene: a combined experimental and theoretical study |
Authors of publication | Böserle, Jiří; Zhigulin, Grigory; Štěpnička, Petr; Horký, Filip; Erben, Milan; Jambor, Roman; R°užička, Aleš; Ketkov, Sergey; Dostál, Libor |
Journal of publication | Dalton Transactions |
Year of publication | 2017 |
Journal volume | 46 |
Journal issue | 36 |
Pages of publication | 12339 - 12353 |
a | 15.39 ± 0.0007 Å |
b | 18.312 ± 0.002 Å |
c | 36.856 ± 0.005 Å |
α | 91.094 ± 0.011° |
β | 97.193 ± 0.005° |
γ | 91.257 ± 0.008° |
Cell volume | 10300.1 ± 1.9 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1318 |
Residual factor for significantly intense reflections | 0.0669 |
Weighted residual factors for significantly intense reflections | 0.1114 |
Weighted residual factors for all reflections included in the refinement | 0.1375 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.115 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/1546890.html
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structural data.