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Information card for entry 1546891
Preview
Coordinates | 1546891.cif |
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Original paper (by DOI) | HTML |
Formula | C63 H81 B2 Ge2 N6 |
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Calculated formula | C63 H81 B2 Ge2 N6 |
Title of publication | Facile activation of alkynes with a boraguanidinato-stabilized germylene: a combined experimental and theoretical study |
Authors of publication | Böserle, Jiří; Zhigulin, Grigory; Štěpnička, Petr; Horký, Filip; Erben, Milan; Jambor, Roman; R°užička, Aleš; Ketkov, Sergey; Dostál, Libor |
Journal of publication | Dalton Transactions |
Year of publication | 2017 |
Journal volume | 46 |
Journal issue | 36 |
Pages of publication | 12339 - 12353 |
a | 22.5261 ± 0.0014 Å |
b | 13.268 ± 0.0015 Å |
c | 21.209 ± 0.002 Å |
α | 90° |
β | 112.06 ± 0.009° |
γ | 90° |
Cell volume | 5874.8 ± 1 Å3 |
Cell temperature | 150 ± 1 K |
Ambient diffraction temperature | 150 ± 1 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0964 |
Residual factor for significantly intense reflections | 0.0476 |
Weighted residual factors for significantly intense reflections | 0.0807 |
Weighted residual factors for all reflections included in the refinement | 0.1018 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.147 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/1546891.html
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