Information card for entry 1550225

Structure parameters

• Formula: C80 H140 K4 N4 O14 Si4
• Calculated formula: C80 H140 K4 N4 O14 Si4
• SMILES: [Si]([O]1[Si](N([K]1)c1c(cccc1C(C)C)C(C)C)(C)C)(N([K]12345[O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6)c1c(cccc1C(C)C)C(C)C)(C)C
• Title of publication: Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds
• Authors of publication: Anker, Mathew; Lein, Matthias; Coles, Martyn P.
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 11.7068 ± 0.0004 Å
• b: 13.9065 ± 0.0004 Å
• c: 14.2431 ± 0.0004 Å
• α: 93.271 ± 0.002°
• β: 99.115 ± 0.002°
• γ: 95.176 ± 0.002°
• Cell volume: 2274.16 ± 0.12 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0604
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1165
• Weighted residual factors for all reflections included in the refinement: 0.1262
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No