Information card for entry 1550226

Structure parameters

• Formula: C28 H46 Cl2 In K N2 O Si2
• Calculated formula: C28 H46 Cl2 In K N2 O Si2
• Title of publication: Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds
• Authors of publication: Anker, Mathew; Lein, Matthias; Coles, Martyn P.
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 18.8952 ± 0.0004 Å
• b: 13.1861 ± 0.0002 Å
• c: 27.8641 ± 0.0005 Å
• α: 90°
• β: 100.042 ± 0.0019°
• γ: 90°
• Cell volume: 6836.1 ± 0.2 ų
• Cell temperature: 119.99 ± 0.1 K
• Ambient diffraction temperature: 119.99 ± 0.1 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0277
• Residual factor for significantly intense reflections: 0.0248
• Weighted residual factors for significantly intense reflections: 0.0648
• Weighted residual factors for all reflections included in the refinement: 0.0668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.012
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No