Information card for entry 1550228

Structure parameters

• Formula: C36 H66 K2 N2 O3 Si2
• Calculated formula: C36 H66 K2 N2 O3 Si2
• Title of publication: Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds
• Authors of publication: Anker, Mathew; Lein, Matthias; Coles, Martyn P.
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 10.0422 ± 0.0004 Å
• b: 11.962 ± 0.0006 Å
• c: 17.7445 ± 0.001 Å
• α: 93.171 ± 0.004°
• β: 96.478 ± 0.004°
• γ: 92.102 ± 0.004°
• Cell volume: 2112.72 ± 0.18 ų
• Cell temperature: 120.01 ± 0.1 K
• Ambient diffraction temperature: 120.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1066
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.1375
• Weighted residual factors for all reflections included in the refinement: 0.1593
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No