Information card for entry 1550229

Structure parameters

• Formula: C59 H99 In2 K2 N4 O2 Si4
• Calculated formula: C59 H99 In2 K2 N4 O2 Si4
• Title of publication: Reduction of Organic Azides by Indyl-Anions. Isolation and Reactivity Studies of Indium-Nitrogen Multiple Bonds
• Authors of publication: Anker, Mathew; Lein, Matthias; Coles, Martyn P.
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 23.2852 ± 0.0003 Å
• b: 17.27697 ± 0.00018 Å
• c: 36.472 ± 0.0005 Å
• α: 90°
• β: 108.506 ± 0.0014°
• γ: 90°
• Cell volume: 13913.9 ± 0.3 ų
• Cell temperature: 120 ± 0.1 K
• Ambient diffraction temperature: 120 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.0464
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1034
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No