Crystallography Open Database

Information card for entry 1551148

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Coordinates	1551148.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H69 N3 Si5
Calculated formula	C40 H69 N3 Si5
Title of publication	A Vinyl Silylsilylene and its Activation of Strong Homo- and Heteroatomic Bonds
Authors of publication	Roy, Matthew M. D.; Ferguson, Michael J.; McDonald, Robert; Zhou, Yuqiao; Rivard, Eric
Journal of publication	Chemical Science
Year of publication	2019
a	11.361 ± 0.0002 Å
b	18.2937 ± 0.0004 Å
c	11.6759 ± 0.0002 Å
α	90°
β	105.758 ± 0.0008°
γ	90°
Cell volume	2335.45 ± 0.08 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.0825
Residual factor for significantly intense reflections	0.0786
Weighted residual factors for significantly intense reflections	0.2237
Weighted residual factors for all reflections included in the refinement	0.2282
Goodness-of-fit parameter for all reflections included in the refinement	1.01
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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