Information card for entry 1552182

Structure parameters

• Formula: C74 H109 N6 Na O38 Sn6
• Calculated formula: C68 H78 N6 Na O32 Sn6
• Title of publication: Assembly of High-Nuclearity Sn26, Sn34-Oxo Clusters: Solvent Strategy and Inorganic Sn Incorporation
• Authors of publication: Zhu, Yu; Zhang, Lei; Zhang, Jian
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 12.9255 ± 0.0002 Å
• b: 19.9189 ± 0.0002 Å
• c: 18.8428 ± 0.0003 Å
• α: 90°
• β: 95.488 ± 0.001°
• γ: 90°
• Cell volume: 4829.06 ± 0.12 ų
• Cell temperature: 297.25 ± 0.1 K
• Ambient diffraction temperature: 297.25 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0652
• Weighted residual factors for significantly intense reflections: 0.1439
• Weighted residual factors for all reflections included in the refinement: 0.1518
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No