Crystallography Open Database

Information card for entry 1552183

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Coordinates	1552183.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C158 H340 Cl12 N8 O92 Sn30
Calculated formula	C152 H266 Cl12 N8 O76 Sn30
Title of publication	Assembly of High-Nuclearity Sn26, Sn34-Oxo Clusters: Solvent Strategy and Inorganic Sn Incorporation
Authors of publication	Zhu, Yu; Zhang, Lei; Zhang, Jian
Journal of publication	Chemical Science
Year of publication	2019
a	16.627 ± 0.003 Å
b	19.217 ± 0.004 Å
c	24.646 ± 0.006 Å
α	87.755 ± 0.008°
β	84.536 ± 0.009°
γ	65.502 ± 0.006°
Cell volume	7133 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1033
Residual factor for significantly intense reflections	0.0768
Weighted residual factors for significantly intense reflections	0.1458
Weighted residual factors for all reflections included in the refinement	0.1571
Goodness-of-fit parameter for all reflections included in the refinement	1.08
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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