Information card for entry 1552453

Structure parameters

• Formula: C34 H41 N2 P3
• Calculated formula: C34 H41 N2 P3
• Title of publication: Direct functionalization of white phosphorus with anionic dicarbenes and mesoionic carbenes: Facile access to 1,2,3-triphosphol-2-ides
• Authors of publication: Ghadwal, Rajendra S.; Rottschäfer, Dennis; Blomeyer, Sebastian; Neumann, Beate; Stammler, Georg
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 10.855 ± 0.0003 Å
• b: 15.5962 ± 0.0003 Å
• c: 19.1059 ± 0.0004 Å
• α: 90°
• β: 102.358 ± 0.002°
• γ: 90°
• Cell volume: 3159.62 ± 0.13 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 4
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0521
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.097
• Weighted residual factors for all reflections included in the refinement: 0.1052
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No