Information card for entry 1552454

Structure parameters

• Formula: C38 H39 Mo N2 O5 P3
• Calculated formula: C38 H39 Mo N2 O5 P3
• Title of publication: Direct functionalization of white phosphorus with anionic dicarbenes and mesoionic carbenes: Facile access to 1,2,3-triphosphol-2-ides
• Authors of publication: Ghadwal, Rajendra S.; Rottschäfer, Dennis; Blomeyer, Sebastian; Neumann, Beate; Stammler, Georg
• Journal of publication: Chemical Science
• Year of publication: 2019
• a: 12.6802 ± 0.0001 Å
• b: 13.7259 ± 0.0001 Å
• c: 23.021 ± 0.0002 Å
• α: 93.562 ± 0.001°
• β: 101.027 ± 0.001°
• γ: 98.039 ± 0.001°
• Cell volume: 3877.8 ± 0.06 ų
• Cell temperature: 100.01 ± 0.1 K
• Ambient diffraction temperature: 100.01 ± 0.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0356
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for significantly intense reflections: 0.0619
• Weighted residual factors for all reflections included in the refinement: 0.0652
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No