Information card for entry 1553616

Structure parameters

• Formula: C22 H24 S4 Si2
• Calculated formula: C22 H24 S4 Si2
• SMILES: s1cc2c3c(c4c(scc4c4c(csc4)c2c1[Si](C)(C)C)[Si](C)(C)C)csc3
• Title of publication: Selective deprotonation of tetra[3,4]thienylene in the presence of n-BuLi
• Authors of publication: Li, Lu; Li, Bingbing; Li, Chunli; Ma, Zhiying; Xu, Li; Wang, Hua
• Journal of publication: Organic Chemistry Frontiers
• Year of publication: 2017
• Journal volume: 4
• Journal issue: 6
• Pages of publication: 1019
• a: 10.5479 ± 0.0013 Å
• b: 16.6 ± 0.002 Å
• c: 13.9079 ± 0.0017 Å
• α: 90°
• β: 92.242 ± 0.002°
• γ: 90°
• Cell volume: 2433.3 ± 0.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0597
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1207
• Weighted residual factors for all reflections included in the refinement: 0.1333
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No