Information card for entry 1555089

Structure parameters

• Formula: C38 H34 P2
• Calculated formula: C38 H34 P2
• SMILES: P12P3C(=C(C(=C3c3ccccc3)C)C)[C@H]([C@@H](C2=C(C(=C1c1ccccc1)C)C)c1ccccc1)c1ccccc1.P12P3C(=C(C(=C3c3ccccc3)C)C)[C@@H]([C@H](C2=C(C(=C1c1ccccc1)C)C)c1ccccc1)c1ccccc1
• Title of publication: Reaction of Phospholes with Aldimines: A One-Step Synthesis of Chelating, Alpha-C2-Bridged Biphospholes.
• Authors of publication: Hu, Zhengsong; Li, Zongyang; Zhao, Kang; Tian, Rongqiang; Duan, Zheng; Mathey, François
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 14
• Pages of publication: 3518 - 3520
• a: 8.6263 ± 0.0009 Å
• b: 12.097 ± 0.002 Å
• c: 16.023 ± 0.006 Å
• α: 107.86 ± 0.03°
• β: 95.73 ± 0.03°
• γ: 104.279 ± 0.013°
• Cell volume: 1514.1 ± 0.7 ų
• Cell temperature: 291 ± 2 K
• Ambient diffraction temperature: 291.15 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0461
• Residual factor for significantly intense reflections: 0.0393
• Weighted residual factors for significantly intense reflections: 0.1078
• Weighted residual factors for all reflections included in the refinement: 0.1148
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No