Information card for entry 1555325

Structure parameters

• Common name: 12mem_dimer
• Formula: C17 H31 Si
• Calculated formula: C17 H31 Si
• Title of publication: Oxidative Dimerization of Silylallenes via Activation of the Allenic C(sp(2))-H Bond Catalyzed by Copper(I) Chloride and N-Hydroxyphthalimide.
• Authors of publication: Sabbasani, Venkata R.; Lee, Daesung
• Journal of publication: Organic letters
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 19
• Pages of publication: 4878 - 4881
• a: 6.5951 ± 0.0014 Å
• b: 11.238 ± 0.003 Å
• c: 12.03 ± 0.003 Å
• α: 105.996 ± 0.006°
• β: 93.545 ± 0.006°
• γ: 94.888 ± 0.006°
• Cell volume: 850.6 ± 0.4 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0807
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1526
• Weighted residual factors for all reflections included in the refinement: 0.1784
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation wavelength: 0.71073 Å
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No