Crystallography Open Database

Information card for entry 1555326

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Coordinates	1555326.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C13 H23 Si
Calculated formula	C13 H23 Si
Title of publication	Oxidative Dimerization of Silylallenes via Activation of the Allenic C(sp(2))-H Bond Catalyzed by Copper(I) Chloride and N-Hydroxyphthalimide.
Authors of publication	Sabbasani, Venkata R.; Lee, Daesung
Journal of publication	Organic letters
Year of publication	2015
Journal volume	17
Journal issue	19
Pages of publication	4878 - 4881
a	6.2702 ± 0.0009 Å
b	10.955 ± 0.0019 Å
c	11.088 ± 0.0019 Å
α	75.965 ± 0.005°
β	74.11 ± 0.005°
γ	74.699 ± 0.005°
Cell volume	694.6 ± 0.2 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1155
Residual factor for significantly intense reflections	0.0964
Weighted residual factors for significantly intense reflections	0.3005
Weighted residual factors for all reflections included in the refinement	0.3182
Goodness-of-fit parameter for all reflections included in the refinement	2.442
Diffraction radiation wavelength	0.71073 Å
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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