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Information card for entry 1555687
Preview
Coordinates | 1555687.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H23 N O2 |
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Calculated formula | C16 H23 N O2 |
SMILES | O=C1N([C@]23[C@H](CC1)[C@H](CC(=O)C2)C[C@H](C3)C)CC=C |
Title of publication | Protecting-Group-Free Total Synthesis of (-)-Lycopodine via Phosphoric Acid Promoted Alkyne Aza-Prins Cyclization. |
Authors of publication | Ma, Donghui; Zhong, Zhuliang; Liu, Zaimin; Zhang, Mingjie; Xu, Shiyan; Xu, Dengyu; Song, Dengpeng; Xie, Xingang; She, Xuegong |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 17 |
Pages of publication | 4328 - 4331 |
a | 7.4804 ± 0.00011 Å |
b | 10.4902 ± 0.00019 Å |
c | 18.4048 ± 0.0003 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 1444.24 ± 0.04 Å3 |
Cell temperature | 294.1 ± 0.5 K |
Ambient diffraction temperature | 294.1 ± 0.5 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0522 |
Residual factor for significantly intense reflections | 0.0513 |
Weighted residual factors for significantly intense reflections | 0.1299 |
Weighted residual factors for all reflections included in the refinement | 0.1317 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.107 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555687.html
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Users of the data should acknowledge the original authors of the
structural data.