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Information card for entry 1555688
Preview
Coordinates | 1555688.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C16 H23 N O2 |
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Calculated formula | C16 H23 N O2 |
Title of publication | Protecting-Group-Free Total Synthesis of (-)-Lycopodine via Phosphoric Acid Promoted Alkyne Aza-Prins Cyclization. |
Authors of publication | Ma, Donghui; Zhong, Zhuliang; Liu, Zaimin; Zhang, Mingjie; Xu, Shiyan; Xu, Dengyu; Song, Dengpeng; Xie, Xingang; She, Xuegong |
Journal of publication | Organic letters |
Year of publication | 2016 |
Journal volume | 18 |
Journal issue | 17 |
Pages of publication | 4328 - 4331 |
a | 10.9468 ± 0.0004 Å |
b | 13.1316 ± 0.0005 Å |
c | 19.8805 ± 0.0008 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 2857.8 ± 0.19 Å3 |
Cell temperature | 296.71 ± 0.1 K |
Ambient diffraction temperature | 296.71 ± 0.1 K |
Number of distinct elements | 4 |
Space group number | 19 |
Hermann-Mauguin space group symbol | P 21 21 21 |
Hall space group symbol | P 2ac 2ab |
Residual factor for all reflections | 0.0442 |
Residual factor for significantly intense reflections | 0.0395 |
Weighted residual factors for significantly intense reflections | 0.0987 |
Weighted residual factors for all reflections included in the refinement | 0.1037 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.056 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1555688.html
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Users of the data should acknowledge the original authors of the
structural data.