Information card for entry 1556439

Structure parameters

• Formula: C42 H84 Cr K N4 O8 Si4
• Calculated formula: C42 H84 Cr K N4 O8 Si4
• Title of publication: Reduction of 2,2'-Bipyridine by Quasi-Linear 3d-Metal(I) Silylamides-A Structural and Spectroscopic Study
• Authors of publication: Muller, I.; Schneider, C.; Pietzonka, C.; Kraus, F.; Werncke, C.G.
• Journal of publication: Inorganics
• Year of publication: 2019
• Journal volume: 7
• Pages of publication: 117
• a: 11.6269 ± 0.0002 Å
• b: 21.5546 ± 0.0004 Å
• c: 21.856 ± 0.0004 Å
• α: 95.633 ± 0.002°
• β: 89.892 ± 0.001°
• γ: 90.377 ± 0.002°
• Cell volume: 5450.83 ± 0.17 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0675
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1447
• Weighted residual factors for all reflections included in the refinement: 0.1502
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No