Information card for entry 1556440

Structure parameters

• Formula: C42 H84 Fe K N4 O8 Si4
• Calculated formula: C42 H84 Fe K N4 O8 Si4
• Title of publication: Reduction of 2,2'-Bipyridine by Quasi-Linear 3d-Metal(I) Silylamides-A Structural and Spectroscopic Study
• Authors of publication: Muller, I.; Schneider, C.; Pietzonka, C.; Kraus, F.; Werncke, C.G.
• Journal of publication: Inorganics
• Year of publication: 2019
• Journal volume: 7
• Pages of publication: 117
• a: 10.8613 ± 0.0005 Å
• b: 13.2627 ± 0.0006 Å
• c: 19.8669 ± 0.0009 Å
• α: 77.597 ± 0.001°
• β: 80.062 ± 0.002°
• γ: 83.452 ± 0.002°
• Cell volume: 2744.3 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0384
• Residual factor for significantly intense reflections: 0.028
• Weighted residual factors for significantly intense reflections: 0.0634
• Weighted residual factors for all reflections included in the refinement: 0.0675
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No