Information card for entry 1560611

Structure parameters

• Formula: C22 H18 O18 Pb3
• Calculated formula: C22 H14 O18 Pb3
• Title of publication: Lead(II) coordination polymers based on rigid-flexible 3,5-bis-oxyacetate-benzoic acid: Structural transition driven by temperature control
• Authors of publication: Chen, Yong-Qiang; Tian, Yuan
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2017
• Journal volume: 247
• Pages of publication: 60 - 66
• a: 10.235 ± 0.002 Å
• b: 11.354 ± 0.002 Å
• c: 12.597 ± 0.003 Å
• α: 88.53 ± 0.03°
• β: 74.14 ± 0.03°
• γ: 67.91 ± 0.03°
• Cell volume: 1299.9 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.056
• Weighted residual factors for significantly intense reflections: 0.1393
• Weighted residual factors for all reflections included in the refinement: 0.155
• Goodness-of-fit parameter for all reflections included in the refinement: 0.926
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No