Information card for entry 1560612

Structure parameters

• Formula: C22 H20 O20 Pb4
• Calculated formula: C22 H14 O19 Pb4
• Title of publication: Lead(II) coordination polymers based on rigid-flexible 3,5-bis-oxyacetate-benzoic acid: Structural transition driven by temperature control
• Authors of publication: Chen, Yong-Qiang; Tian, Yuan
• Journal of publication: Journal of Solid State Chemistry
• Year of publication: 2017
• Journal volume: 247
• Pages of publication: 60 - 66
• a: 8.9756 ± 0.0018 Å
• b: 11.556 ± 0.002 Å
• c: 15.721 ± 0.003 Å
• α: 100.02 ± 0.03°
• β: 102.77 ± 0.03°
• γ: 97.23 ± 0.03°
• Cell volume: 1542.9 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0956
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1019
• Weighted residual factors for all reflections included in the refinement: 0.1121
• Goodness-of-fit parameter for all reflections included in the refinement: 0.864
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No