Information card for entry 1565366

Structure parameters

• Formula: C14 H42 K0.5 N6.8 Nb6 O138.4 P4 W30
• Calculated formula: C14 H42 K0.5 N6.8 Nb6 O138.4 P4 W30
• Title of publication: Niobium uptake by {P2W12} polyoxoanion with [NbO(C2O4)2(H2O)2]− as Nb source
• Authors of publication: Shmakova, Alexandra A.; Sukhikh, Taisiya S.; Volchek, Victoria V.; Yanshole, Vadim; Stass, Dmitri V.; Filatov, Eugeniy Yu.; Glebov, Eugeniy M.; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2020
• Journal volume: 502
• Pages of publication: 119319
• a: 13.5004 ± 0.0003 Å
• b: 23.0057 ± 0.0008 Å
• c: 27.1162 ± 0.0008 Å
• α: 100.927 ± 0.003°
• β: 96.488 ± 0.002°
• γ: 105.419 ± 0.002°
• Cell volume: 7851.9 ± 0.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1504
• Residual factor for significantly intense reflections: 0.0789
• Weighted residual factors for significantly intense reflections: 0.1956
• Weighted residual factors for all reflections included in the refinement: 0.2235
• Goodness-of-fit parameter for all reflections included in the refinement: 1.085
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No