Information card for entry 1565367

Structure parameters

• Formula: C16 N8 Nb6.4 O144.78 P4 W29.6
• Calculated formula: C16 N8 Nb6.4 O144.78 P4 W29.6
• Title of publication: Niobium uptake by {P2W12} polyoxoanion with [NbO(C2O4)2(H2O)2]− as Nb source
• Authors of publication: Shmakova, Alexandra A.; Sukhikh, Taisiya S.; Volchek, Victoria V.; Yanshole, Vadim; Stass, Dmitri V.; Filatov, Eugeniy Yu.; Glebov, Eugeniy M.; Abramov, Pavel A.; Sokolov, Maxim N.
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2020
• Journal volume: 502
• Pages of publication: 119319
• a: 19.5879 ± 0.0012 Å
• b: 21.9143 ± 0.0013 Å
• c: 18.3017 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 7856.1 ± 0.8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 58
• Hermann-Mauguin space group symbol: P n n m
• Hall space group symbol: -P 2 2n
• Residual factor for all reflections: 0.048
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.08
• Weighted residual factors for all reflections included in the refinement: 0.0904
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No