Information card for entry 1566526

Structure parameters

• Formula: C78 H116 Ga2 N6 Sb2 Si
• Calculated formula: C78 H116 Ga2 N6 Sb2 Si
• Title of publication: Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides
• Authors of publication: Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 10.919 ± 0.002 Å
• b: 14.343 ± 0.003 Å
• c: 26.014 ± 0.006 Å
• α: 83.994 ± 0.015°
• β: 78.718 ± 0.01°
• γ: 88.053 ± 0.01°
• Cell volume: 3973 ± 1.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0628
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0841
• Weighted residual factors for all reflections included in the refinement: 0.0942
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No