Information card for entry 1566527

Structure parameters

• Formula: C64.5 H98 Cl2 Ga2 N4 Sb2 Si
• Calculated formula: C64.5 H98 Cl2 Ga2 N4 Sb2 Si
• Title of publication: Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides
• Authors of publication: Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 19.7547 ± 0.0017 Å
• b: 10.5843 ± 0.0009 Å
• c: 33.512 ± 0.003 Å
• α: 90°
• β: 96.97 ± 0.004°
• γ: 90°
• Cell volume: 6955.2 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0454
• Residual factor for significantly intense reflections: 0.0359
• Weighted residual factors for significantly intense reflections: 0.0847
• Weighted residual factors for all reflections included in the refinement: 0.0902
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No