Syntheses, homeomorphic and configurational isomerizations, and structures of macrocyclic aliphatic dibridgehead diphosphines; molecules that turn themselves inside out
Authors of publication
Zhu, Yun; Stollenz, Michael; Zarcone, Samuel R.; Kharel, Sugam; Joshi, Hemant; Bhuvanesh, Nattamai; Reibenspies, Joseph H.; Gladysz, John A.
Journal of publication
Chemical Science
Year of publication
2022
a
9.1903 ± 0.0019 Å
b
9.1903 ± 0.0019 Å
c
89.58 ± 0.02 Å
α
90°
β
90°
γ
120°
Cell volume
6552 ± 2 Å3
Cell temperature
110 ± 2 K
Ambient diffraction temperature
110.15 K
Number of distinct elements
3
Space group number
167
Hermann-Mauguin space group symbol
R -3 c :H
Hall space group symbol
-R 3 2"c
Residual factor for all reflections
0.0668
Residual factor for significantly intense reflections
0.04
Weighted residual factors for significantly intense reflections
0.0651
Weighted residual factors for all reflections included in the refinement
0.0707
Goodness-of-fit parameter for all reflections included in the refinement
