Information card for entry 1568651

Structure parameters

• Formula: C108 H120 N4 O3 P6 Rh2
• Calculated formula: C108 H120 N4 O3 P6 Rh2
• Title of publication: Probing the donor strength of yldiide ligands: synthesis, structure and reactivity of rhodium complexes with a PC_ylideN pincer ligand.
• Authors of publication: Lapointe, Sébastien; Duari, Prakash; Gessner, Viktoria H.
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 14
• Pages of publication: 3816 - 3825
• a: 13.4359 ± 0.0002 Å
• b: 14.5922 ± 0.0002 Å
• c: 28.2841 ± 0.0004 Å
• α: 83.805 ± 0.001°
• β: 82.158 ± 0.001°
• γ: 65.89 ± 0.002°
• Cell volume: 5005.91 ± 0.15 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0443
• Weighted residual factors for significantly intense reflections: 0.1194
• Weighted residual factors for all reflections included in the refinement: 0.1216
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No