Information card for entry 1568652

Structure parameters

• Formula: C53 H59 I N2 O P3 Rh
• Calculated formula: C53 H59 I N2 O P3 Rh
• Title of publication: Probing the donor strength of yldiide ligands: synthesis, structure and reactivity of rhodium complexes with a PC_ylideN pincer ligand.
• Authors of publication: Lapointe, Sébastien; Duari, Prakash; Gessner, Viktoria H.
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 14
• Pages of publication: 3816 - 3825
• a: 43.4288 ± 0.0005 Å
• b: 43.4288 ± 0.0005 Å
• c: 13.10301 ± 0.00016 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 21402.1 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0573
• Residual factor for significantly intense reflections: 0.0506
• Weighted residual factors for significantly intense reflections: 0.1252
• Weighted residual factors for all reflections included in the refinement: 0.1292
• Goodness-of-fit parameter for all reflections included in the refinement: 1.11
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No