Information card for entry 1569006

Structure parameters

• Formula: C47 H62 Cl2 Ge N3
• Calculated formula: C47 H62 Cl2 Ge N3
• Title of publication: A crystalline T-shaped planar group 14 anion.
• Authors of publication: Liu, Xiaona; Dai, Yuyang; Bao, Manling; Wang, Wenjuan; Li, Qianli; Liu, Chunmeng; Wang, Xinping; Su, Yuanting
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 21
• Pages of publication: 5722 - 5727
• a: 31.6991 ± 0.0018 Å
• b: 18.5153 ± 0.0009 Å
• c: 15.1604 ± 0.0008 Å
• α: 90°
• β: 94.55 ± 0.002°
• γ: 90°
• Cell volume: 8869.9 ± 0.8 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120.06 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0535
• Residual factor for significantly intense reflections: 0.0428
• Weighted residual factors for significantly intense reflections: 0.1101
• Weighted residual factors for all reflections included in the refinement: 0.1172
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0575
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No