Information card for entry 1569007

Structure parameters

• Formula: C51 H72 Ge N3
• Calculated formula: C51 H72 Ge N3
• Title of publication: A crystalline T-shaped planar group 14 anion.
• Authors of publication: Liu, Xiaona; Dai, Yuyang; Bao, Manling; Wang, Wenjuan; Li, Qianli; Liu, Chunmeng; Wang, Xinping; Su, Yuanting
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 21
• Pages of publication: 5722 - 5727
• a: 12.7334 ± 0.0007 Å
• b: 13.204 ± 0.003 Å
• c: 14.396 ± 0.0006 Å
• α: 98.596 ± 0.005°
• β: 101.664 ± 0.003°
• γ: 96.759 ± 0.006°
• Cell volume: 2316.3 ± 0.6 ų
• Cell temperature: 120 K
• Ambient diffraction temperature: 120 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0398
• Residual factor for significantly intense reflections: 0.0383
• Weighted residual factors for significantly intense reflections: 0.0995
• Weighted residual factors for all reflections included in the refinement: 0.1008
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 1.34138 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No