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Information card for entry 1569904
Preview
Coordinates | 1569904.cif |
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Original paper (by DOI) | HTML |
Formula | C58 H44 N2 O8 S2 |
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Calculated formula | C58 H44 N2 O8 S2 |
Title of publication | Asymmetric Friedel-Crafts reaction of unsaturated carbonyl-tethered heteroarenes <i>via</i> vinylogous activation of Pd<sup>0</sup>-π-Lewis base catalysis. |
Authors of publication | Jiang, Bo; Gui, Wu-Tao; Wang, Hao-Tian; Xie, Ke; Chen, Zhi-Chao; Zhu, Lei; Ouyang, Qin; Du, Wei; Chen, Ying-Chun |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 39 |
Pages of publication | 10867 - 10874 |
a | 32.1431 ± 0.0008 Å |
b | 7.189 ± 0.0002 Å |
c | 11.8007 ± 0.0003 Å |
α | 90° |
β | 98.963 ± 0.002° |
γ | 90° |
Cell volume | 2693.57 ± 0.12 Å3 |
Cell temperature | 302 ± 2 K |
Ambient diffraction temperature | 302 K |
Number of distinct elements | 5 |
Space group number | 5 |
Hermann-Mauguin space group symbol | C 1 2 1 |
Hall space group symbol | C 2y |
Residual factor for all reflections | 0.0554 |
Residual factor for significantly intense reflections | 0.0425 |
Weighted residual factors for significantly intense reflections | 0.1046 |
Weighted residual factors for all reflections included in the refinement | 0.1151 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.066 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1569904.html
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Users of the data should acknowledge the original authors of the
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