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Information card for entry 1569905
Preview
Coordinates | 1569905.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C37 H25 Cl3 N2 O4 |
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Calculated formula | C37 H25 Cl3 N2 O4 |
Title of publication | Asymmetric Friedel-Crafts reaction of unsaturated carbonyl-tethered heteroarenes <i>via</i> vinylogous activation of Pd<sup>0</sup>-π-Lewis base catalysis. |
Authors of publication | Jiang, Bo; Gui, Wu-Tao; Wang, Hao-Tian; Xie, Ke; Chen, Zhi-Chao; Zhu, Lei; Ouyang, Qin; Du, Wei; Chen, Ying-Chun |
Journal of publication | Chemical science |
Year of publication | 2023 |
Journal volume | 14 |
Journal issue | 39 |
Pages of publication | 10867 - 10874 |
a | 13.2537 ± 0.0004 Å |
b | 8.0062 ± 0.0002 Å |
c | 15.7406 ± 0.0005 Å |
α | 90° |
β | 94.626 ± 0.001° |
γ | 90° |
Cell volume | 1664.82 ± 0.08 Å3 |
Cell temperature | 273 ± 2 K |
Ambient diffraction temperature | 273.15 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1003 |
Residual factor for significantly intense reflections | 0.0667 |
Weighted residual factors for significantly intense reflections | 0.1763 |
Weighted residual factors for all reflections included in the refinement | 0.2034 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.036 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1569905.html
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