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Information card for entry 1570696
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Coordinates | 1570696.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H24 B N O2 |
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Calculated formula | C22 H24 B N O2 |
Title of publication | Ligand-controlled regiodivergent Ni-catalyzed <i>trans</i>-hydroboration/carboboration of internal alkynes with B<sub>2</sub>pin<sub>2</sub>. |
Authors of publication | Chen, Zunsheng; Nie, Biao; Li, Xiaoning; Liu, Teng; Li, Chunsheng; Huang, Jiuzhong |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 6 |
Pages of publication | 2236 - 2242 |
a | 10.1597 ± 0.0002 Å |
b | 10.2937 ± 0.0002 Å |
c | 11.2498 ± 0.0003 Å |
α | 79.933 ± 0.002° |
β | 89.723 ± 0.002° |
γ | 76.12 ± 0.002° |
Cell volume | 1123.73 ± 0.04 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0665 |
Residual factor for significantly intense reflections | 0.0649 |
Weighted residual factors for significantly intense reflections | 0.1629 |
Weighted residual factors for all reflections included in the refinement | 0.1641 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.065 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1570696.html
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