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Information card for entry 1570697
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Coordinates | 1570697.cif |
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Original paper (by DOI) | HTML |
Formula | C22 H24 B N O2 |
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Calculated formula | C22 H24 B N O2 |
Title of publication | Ligand-controlled regiodivergent Ni-catalyzed <i>trans</i>-hydroboration/carboboration of internal alkynes with B<sub>2</sub>pin<sub>2</sub>. |
Authors of publication | Chen, Zunsheng; Nie, Biao; Li, Xiaoning; Liu, Teng; Li, Chunsheng; Huang, Jiuzhong |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 6 |
Pages of publication | 2236 - 2242 |
a | 9.6547 ± 0.001 Å |
b | 10.2621 ± 0.0013 Å |
c | 10.6861 ± 0.0015 Å |
α | 102.169 ± 0.011° |
β | 105.217 ± 0.01° |
γ | 103.684 ± 0.01° |
Cell volume | 949.7 ± 0.2 Å3 |
Cell temperature | 150 ± 0.1 K |
Ambient diffraction temperature | 150 ± 0.1 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0626 |
Residual factor for significantly intense reflections | 0.0498 |
Weighted residual factors for significantly intense reflections | 0.1141 |
Weighted residual factors for all reflections included in the refinement | 0.1232 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.076 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/1570697.html
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