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Information card for entry 1571042
Preview
| Coordinates | 1571042.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H94 K N O8 Si2 |
|---|---|
| Calculated formula | C44 H94 K N O8 Si2 |
| Title of publication | s-Block metal complexes of superbulky (<sup><i>t</i></sup>Bu<sub>3</sub>Si)<sub>2</sub>N<sup>-</sup>: a new weakly coordinating anion? |
| Authors of publication | Knüpfer, Christian; Klerner, Lukas; Mai, Jonathan; Langer, Jens; Harder, Sjoerd |
| Journal of publication | Chemical science |
| Year of publication | 2024 |
| Journal volume | 15 |
| Journal issue | 12 |
| Pages of publication | 4386 - 4395 |
| a | 10.782 ± 0.0002 Å |
| b | 15.4196 ± 0.0003 Å |
| c | 23.653 ± 0.0004 Å |
| α | 80.1846 ± 0.0015° |
| β | 78.8889 ± 0.0016° |
| γ | 83.583 ± 0.0015° |
| Cell volume | 3789.53 ± 0.12 Å3 |
| Cell temperature | 100 ± 0.3 K |
| Ambient diffraction temperature | 100 ± 0.3 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0486 |
| Residual factor for significantly intense reflections | 0.042 |
| Weighted residual factors for significantly intense reflections | 0.1123 |
| Weighted residual factors for all reflections included in the refinement | 0.12 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.022 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
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The link is: https://www.crystallography.net/1571042.html
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