Information card for entry 1571043

Structure parameters

• Formula: C24 H54 Cs N Si2
• Calculated formula: C24 H54 Cs N Si2
• Title of publication: s-Block metal complexes of superbulky (^<i>t</i>Bu₃Si)₂N^-: a new weakly coordinating anion?
• Authors of publication: Knüpfer, Christian; Klerner, Lukas; Mai, Jonathan; Langer, Jens; Harder, Sjoerd
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 12
• Pages of publication: 4386 - 4395
• a: 11.47464 ± 0.00007 Å
• b: 11.47464 ± 0.00007 Å
• c: 21.21699 ± 0.00017 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2793.59 ± 0.03 ų
• Cell temperature: 100 ± 0.6 K
• Ambient diffraction temperature: 100 ± 0.6 K
• Number of distinct elements: 5
• Space group number: 92
• Hermann-Mauguin space group symbol: P 41 21 2
• Hall space group symbol: P 4abw 2nw
• Residual factor for all reflections: 0.0179
• Residual factor for significantly intense reflections: 0.0176
• Weighted residual factors for significantly intense reflections: 0.0449
• Weighted residual factors for all reflections included in the refinement: 0.0451
• Goodness-of-fit parameter for all reflections included in the refinement: 1.049
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No