Information card for entry 1571048

Structure parameters

• Formula: C61 H112.49 Mg N3 O2 Si2
• Calculated formula: C61 H112.49 Mg N3 O2 Si2
• Title of publication: s-Block metal complexes of superbulky (^<i>t</i>Bu₃Si)₂N^-: a new weakly coordinating anion?
• Authors of publication: Knüpfer, Christian; Klerner, Lukas; Mai, Jonathan; Langer, Jens; Harder, Sjoerd
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 12
• Pages of publication: 4386 - 4395
• a: 16.7968 ± 0.0004 Å
• b: 16.8461 ± 0.0003 Å
• c: 23.1147 ± 0.0005 Å
• α: 90°
• β: 106.935 ± 0.002°
• γ: 90°
• Cell volume: 6256.9 ± 0.2 ų
• Cell temperature: 99.97 ± 0.11 K
• Ambient diffraction temperature: 99.97 ± 0.11 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.063
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.1614
• Weighted residual factors for all reflections included in the refinement: 0.1646
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No