Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 1571048
Preview
Coordinates | 1571048.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C61 H112.49 Mg N3 O2 Si2 |
---|---|
Calculated formula | C61 H112.49 Mg N3 O2 Si2 |
Title of publication | s-Block metal complexes of superbulky (<sup><i>t</i></sup>Bu<sub>3</sub>Si)<sub>2</sub>N<sup>-</sup>: a new weakly coordinating anion? |
Authors of publication | Knüpfer, Christian; Klerner, Lukas; Mai, Jonathan; Langer, Jens; Harder, Sjoerd |
Journal of publication | Chemical science |
Year of publication | 2024 |
Journal volume | 15 |
Journal issue | 12 |
Pages of publication | 4386 - 4395 |
a | 16.7968 ± 0.0004 Å |
b | 16.8461 ± 0.0003 Å |
c | 23.1147 ± 0.0005 Å |
α | 90° |
β | 106.935 ± 0.002° |
γ | 90° |
Cell volume | 6256.9 ± 0.2 Å3 |
Cell temperature | 99.97 ± 0.11 K |
Ambient diffraction temperature | 99.97 ± 0.11 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.063 |
Residual factor for significantly intense reflections | 0.054 |
Weighted residual factors for significantly intense reflections | 0.1614 |
Weighted residual factors for all reflections included in the refinement | 0.1646 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.128 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/1571048.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.