Information card for entry 1571049

Structure parameters

• Formula: C40 H86 Li N O8 Si2
• Calculated formula: C40 H86 Li N O8 Si2
• Title of publication: s-Block metal complexes of superbulky (^<i>t</i>Bu₃Si)₂N^-: a new weakly coordinating anion?
• Authors of publication: Knüpfer, Christian; Klerner, Lukas; Mai, Jonathan; Langer, Jens; Harder, Sjoerd
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 12
• Pages of publication: 4386 - 4395
• a: 20.1279 ± 0.0003 Å
• b: 26.8869 ± 0.0004 Å
• c: 17.1171 ± 0.0003 Å
• α: 90°
• β: 90.741 ± 0.002°
• γ: 90°
• Cell volume: 9262.6 ± 0.3 ų
• Cell temperature: 100 ± 0.4 K
• Ambient diffraction temperature: 100 ± 0.4 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.062
• Residual factor for significantly intense reflections: 0.0562
• Weighted residual factors for significantly intense reflections: 0.1518
• Weighted residual factors for all reflections included in the refinement: 0.1566
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No