Information card for entry 1571394

Structure parameters

• Formula: C56 H90 Si
• Calculated formula: C56 H90 Si
• Title of publication: Approach to the “Missing” Diarylsilylene: Formation, Characterization, and Intramolecular C–H Bond Activation of Blue Diarylsilylenes with Bulky Rind Groups
• Authors of publication: Mochihara, Kazuki; Morimoto, Tatsuto; Ota, Kei; Marumoto, Shinsuke; Hashizume, Daisuke; Matsuo, Tsukasa
• Journal of publication: International Journal of Molecular Sciences
• Year of publication: 2024
• Journal volume: 25
• Journal issue: 7
• Pages of publication: 3761
• a: 10.1298 ± 0.0006 Å
• b: 10.14 ± 0.0006 Å
• c: 24.4558 ± 0.0013 Å
• α: 84.557 ± 0.005°
• β: 85.566 ± 0.005°
• γ: 78.612 ± 0.005°
• Cell volume: 2447 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 3
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1496
• Residual factor for significantly intense reflections: 0.0768
• Weighted residual factors for significantly intense reflections: 0.163
• Weighted residual factors for all reflections included in the refinement: 0.1914
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No