Information card for entry 1571395

Structure parameters

• Formula: C56 H90 Si
• Calculated formula: C56 H90 Si
• Title of publication: Approach to the “Missing” Diarylsilylene: Formation, Characterization, and Intramolecular C–H Bond Activation of Blue Diarylsilylenes with Bulky Rind Groups
• Authors of publication: Mochihara, Kazuki; Morimoto, Tatsuto; Ota, Kei; Marumoto, Shinsuke; Hashizume, Daisuke; Matsuo, Tsukasa
• Journal of publication: International Journal of Molecular Sciences
• Year of publication: 2024
• Journal volume: 25
• Journal issue: 7
• Pages of publication: 3761
• a: 32.72 ± 0.007 Å
• b: 18.594 ± 0.004 Å
• c: 16.662 ± 0.004 Å
• α: 90°
• β: 104.756 ± 0.003°
• γ: 90°
• Cell volume: 9803 ± 4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 3
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0969
• Residual factor for significantly intense reflections: 0.0757
• Weighted residual factors for significantly intense reflections: 0.1704
• Weighted residual factors for all reflections included in the refinement: 0.1823
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No