Information card for entry 1571929

Structure parameters

• Formula: C42 H99 Mo10 N5 O36 Th
• Calculated formula: C42 H99 Mo10 N5 O36 Th
• Title of publication: Leveraging a reduced polyoxomolybdate-alkoxide cluster for the formation of a stable U(v) sandwich complex.
• Authors of publication: Shiels, Dominic; Brennessel, William W.; Crawley, Matthew R.; Matson, Ellen M.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 28
• Pages of publication: 11072 - 11083
• a: 12.8161 ± 0.0002 Å
• b: 15.4649 ± 0.0002 Å
• c: 19.9194 ± 0.0003 Å
• α: 87.176 ± 0.001°
• β: 84.075 ± 0.001°
• γ: 73.714 ± 0.001°
• Cell volume: 3768.5 ± 0.1 ų
• Cell temperature: 100.01 ± 0.16 K
• Ambient diffraction temperature: 100.01 ± 0.16 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0372
• Residual factor for significantly intense reflections: 0.0252
• Weighted residual factors for significantly intense reflections: 0.0507
• Weighted residual factors for all reflections included in the refinement: 0.053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.56087 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No