Information card for entry 1571930

Structure parameters

• Formula: C26.61 H65.22 Cl5.22 Mo10 N3 O36 U
• Calculated formula: C26.609 H65.218 Cl5.218 Mo10 N3 O36 U
• Title of publication: Leveraging a reduced polyoxomolybdate-alkoxide cluster for the formation of a stable U(v) sandwich complex.
• Authors of publication: Shiels, Dominic; Brennessel, William W.; Crawley, Matthew R.; Matson, Ellen M.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 28
• Pages of publication: 11072 - 11083
• a: 16.31 ± 0.0001 Å
• b: 21.2206 ± 0.0001 Å
• c: 18.9017 ± 0.0001 Å
• α: 90°
• β: 103.313 ± 0.001°
• γ: 90°
• Cell volume: 6366.22 ± 0.07 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0404
• Residual factor for significantly intense reflections: 0.0389
• Weighted residual factors for significantly intense reflections: 0.1028
• Weighted residual factors for all reflections included in the refinement: 0.1038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.093
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No