Information card for entry 1572154
| Formula |
C35 H34 N2 O2 |
| Calculated formula |
C35 H34 N2 O2 |
| Title of publication |
Access to distal biaxial atropisomers by iridium catalyzed asymmetric C-H alkylation. |
| Authors of publication |
Hu, Xueqing; Zhao, Yunxu; He, Tong; Niu, Caoyue; Liu, Feipeng; Jia, Wei; Mu, Yi; Li, Xingwei; Rong, Zi-Qiang |
| Journal of publication |
Chemical science |
| Year of publication |
2024 |
| Journal volume |
15 |
| Journal issue |
33 |
| Pages of publication |
13541 - 13549 |
| a |
10.8233 ± 0.0006 Å |
| b |
7.0541 ± 0.0004 Å |
| c |
18.1771 ± 0.001 Å |
| α |
90° |
| β |
94.633 ± 0.002° |
| γ |
90° |
| Cell volume |
1383.26 ± 0.13 Å3 |
| Cell temperature |
193 K |
| Ambient diffraction temperature |
193 K |
| Number of distinct elements |
4 |
| Space group number |
4 |
| Hermann-Mauguin space group symbol |
P 1 21 1 |
| Hall space group symbol |
P 2yb |
| Residual factor for all reflections |
0.0321 |
| Residual factor for significantly intense reflections |
0.0319 |
| Weighted residual factors for significantly intense reflections |
0.0804 |
| Weighted residual factors for all reflections included in the refinement |
0.0807 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.088 |
| Diffraction radiation wavelength |
1.54178 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
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The link is:
https://www.crystallography.net/1572154.html
