Information card for entry 2000021

Structure parameters

• Formula: C65 H137 N13 S8 W6
• Calculated formula: C98 H186 N18 S16 W12
• Title of publication: An Improved High Yield Synthesis Procedure and Reactivity of W~6~S~8~(4-tert-butylpyridine)~6~
• Authors of publication: Venkataraman, D.; Rayburn, Lori L.; Hill, Laurie I.; Jin, Song; Malik, Abds-Sami; Turneau, Kevin J.; DiSalvo, Francis J.
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Journal issue: 4
• Pages of publication: 828 - 830
• a: 19.432 ± 0.004 Å
• b: 19.432 ± 0.004 Å
• c: 22.574 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8524 ų
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.0579
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No