Information card for entry 2000022

Structure parameters

• Formula: C48 H102 P6 S8 W6
• Calculated formula: C240 H504 P36 S40 W36
• Title of publication: An Improved High Yield Synthesis Procedure and Reactivity of W~6~S~8~(4-tert-butylpyridine)~6~
• Authors of publication: Venkataraman, D.; Rayburn, Lori L.; Hill, Laurie I.; Jin, Song; Malik, Abds-Sami; Turneau, Kevin J.; DiSalvo, Francis J.
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Journal issue: 4
• Pages of publication: 828 - 830
• a: 17.481 ± 0.003 Å
• b: 17.481 ± 0.003 Å
• c: 19.935 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5275.69 ų
• Number of distinct elements: 5
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.0402
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No