Crystallography Open Database

Information card for entry 2004988

2004987 << 2004988 >> 2004989

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Coordinates	2004988.cif
Original IUCr paper	HTML

Structure parameters

Formula	C36 H30 Cl3.86 O0.14 P2 Re
Calculated formula	C36 H30 Cl4 O0.666667 P2 Re
Title of publication	<i>trans</i>-Tetrachlorobis(triphenylphosphine-<i>P</i>)rhenium(IV)‒<i>mer</i>-<i>trans</i>-Trichlorooxobis(triphenylphosphine-<i>P</i>)rhenium(V) (0.86/0.14)
Authors of publication	Luo, H.; Orvig, C.; Rettig, S. J.
Journal of publication	Acta Crystallographica Section C
Year of publication	1996
Journal volume	52
Journal issue	6
Pages of publication	1377 - 1380
a	14.204 ± 0.002 Å
b	16.381 ± 0.003 Å
c	11.878 ± 0.002 Å
α	96.13 ± 0.01°
β	92.42 ± 0.01°
γ	64.94 ± 0.01°
Cell volume	2489.2 ± 0.7 Å³
Cell temperature	294.2 K
Ambient diffraction temperature	294.2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for significantly intense reflections	0.032
Weighted residual factors for significantly intense reflections	0.025
Goodness-of-fit parameter for significantly intense reflections	1.24
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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