Information card for entry 2005151

Structure parameters

• Formula: C27 H28 N2 O6 V
• Calculated formula: C28 H28 N2 O7 V
• Title of publication: 5,5'-(2-Hydroxy-1,3-propandiyldiamino)bis(1-phenyl-1,3-hexanedionato-<i>O</i>,<i>O</i>')oxovanadium(IV), [VO(C~27~H~28~N~2~O~5~)]
• Authors of publication: Hope, H.; Borer, L. L.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1996
• Journal volume: 52
• Journal issue: 7
• Pages of publication: 1621 - 1624
• a: 9.36 ± 0.002 Å
• b: 9.845 ± 0.002 Å
• c: 15.216 ± 0.004 Å
• α: 85.18 ± 0.02°
• β: 77.79 ± 0.02°
• γ: 63.75 ± 0.02°
• Cell volume: 1229 ± 0.5 ų
• Cell temperature: 118 ± 1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0908
• Residual factor for significantly intense reflections: 0.065
• Weighted residual factors for all reflections: 0.1668
• Weighted residual factors for significantly intense reflections: 0.147
• Goodness-of-fit parameter for significantly intense reflections: 1.054
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No