Information card for entry 2008371

Structure parameters

• Chemical name: Chlorobis-[1,2-bis(diphenylphosphino)ethane]oxotungsten(IV) hexafluorophospate chloroform solvate
• Formula: C53 H49 Cl4 F6 O P5 W
• Calculated formula: C53 H49 Cl4 F6 O P5 W
• Title of publication: The oxotungsten(IV) complex [WOCl(Ph~2~PCH~2~CH~2~PPh~2~)~2~]PF~6~^.^CHCl~3~
• Authors of publication: Llusar, R.; Mata, J.; Peris, E.; Köckerling, M.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 4
• Pages of publication: 506 - 508
• a: 11.684 ± 0.002 Å
• b: 14.943 ± 0.003 Å
• c: 16.749 ± 0.003 Å
• α: 105.79 ± 0.01°
• β: 106.85 ± 0.01°
• γ: 91.36 ± 0.01°
• Cell volume: 2676.4 ± 0.9 ų
• Cell temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for all reflections included in the refinement: 0.048
• Goodness-of-fit parameter for significantly intense reflections: 1.421
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No