Information card for entry 2010038

Structure parameters

• Chemical name: chloro-(bicyclo[2.2.1]hepta-2,5-diene)-(diazabicyclo[4.3.0]non-5-ene) rhodium(I)
• Formula: C14 H20 Cl N2 Rh
• Calculated formula: C14 H20 Cl N2 Rh
• Title of publication: Rhodium(I) complexes with 1,5-diazabicyclo[4.3.0]non-5-ene (dbn) as a ligand: [RhCl(nbd)(dbn)] (I) and [Rh(dbn)~2~(cod)][PF~6~] (II) (nbd = norbornadiene, cod = 1,5-cyclooctadiene)
• Authors of publication: Flörke, Ulrich; Haupt, Hans-Jürgen
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1994
• Journal volume: 50
• Journal issue: 9
• Pages of publication: 1424 - 1427
• a: 14.139 ± 0.004 Å
• b: 7.378 ± 0.002 Å
• c: 14.855 ± 0.004 Å
• α: 90°
• β: 114.22 ± 0.02°
• γ: 90°
• Cell volume: 1413.2 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0923
• Residual factor for significantly intense reflections: 0.0482
• Weighted residual factors for all reflections: 0.1086
• Weighted residual factors for significantly intense reflections: 0.0909
• Goodness-of-fit parameter for all reflections: 1.03
• Goodness-of-fit parameter for significantly intense reflections: 1.074
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No